About Nauru cathode material energy storage
LMOF03 and LMOF06 were synthesized by mixing stoichiometric Li2MnO3 (obtained by firing Li2CO3 (Alfa Aesar, 99.0%) and MnO2 (Alfa Aesar, 99.9%) at 800 °C in air for 16 h), MnF2 (Alfa Aesar, 99%), Mn2O.
The fabrication of cathode electrodes was done in an argon-filled glove box. The active material (70 wt%) was first manually mixed with Super C65 carbon black (Timcal, 20 wt%).
Elemental analysis was performed by Luvak Inc. using direct-current plasma emission spectroscopy (ASTM E 1097-12) for the metal species and an ion-selective electrode metho.
For the operando XANES experiments, modified coin cells were used with holes in the centre of all the stainless-steel parts and sealed with X-ray transparent Kapton tapes. A galvano.
mRIXS was measured at the iRIXS endstation on Beamline 8.0.1 of the Advanced Light Source in Lawrence Berkeley National Laboratory21. The mapping data we.
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